Appendix
Upgrade path (Section 8)
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Deploy an inert ceramic-metal anode to eliminate residual carbon contact.
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Expand the MOE pot with dual-zone heaters for higher throughput.
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Upgrade spectrometers for deeper UV coverage to resolve trace boron/phosphorus.
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Automate tapping and ladle handling, integrating spectral feedback for closed-loop recipe tuning.
Target setpoints (Appendix A)
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MOE hot-zone: 1625 °C nominal.
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Fe stage: current density 0.2–0.4 A cm⁻², tuned via OES.
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Si stage: increase potential by 10–20 % compared to the Fe stage, watching silicon emission and headspace oxygen.
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Vacuum refining: 1700–1800 °C, ≤10 Pa, 30–90 min hold.
Minimal tools (Appendix B)
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IR thermometer for quick checks.
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Torque drivers, crimp kits, and electrical hand tools.
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TIG-grade gloves, tongs, face shield, and PPE described in the safety chapter.
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Precision scale and sieve set for feed preparation.
Expected consumables per 10 runs (Appendix C)
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Argon: ≤1 m³ with reclaim.
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Liners: 1 primary ZrO₂ liner plus 1 Al₂O₃ backup.
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Anode face or coating: replace as needed if consumable.
Cost recap
The v0.1 build lands at \$8.8–9.8k when leveraging surplus procurement strategies detailed in Materials & Components. Track actual expenses to refine future revisions of the manual.